Furnance Timbangan Digital Mortal Pompa Peristaltik

LAMPIRAN A Gambar Bahan Dan Alat Penelitian Bahan Penelitian Sampel BaNi x Al 6-x Fe 6 O 19 Alat Penelitian Furnance Timbangan Digital Mortal Pompa Peristaltik

Magnetic Stirrer Hot Plate Crussible Magnet Permanen Vial HEM Beaker Glass Oven Mammert Thermometer

Alat XRD Alat VNA Alat SEM-EDS Alat VSM

LAMPIRAN B Stokiometri wt% Sampel BaNi x Al 6-x Fe 6 O 19 Reaksi : BaAl 6 Fe 6 O 19 3Al 2 O 3 + BaCO 3 + 3Fe 2 O 3 -------> BaAl 6 Fe 6 O 19 + CO 2 BaNi 0.5 Al 5.5Fe 6 O 19 5.5Al 2 O 3 +2BaCO 3 +6Fe 2 O 3 +NiO+0.25O 2 -->2BaNi 0.5 Al 5.5 Fe 6 O 19 +2CO 2 BaNiAl 5 Fe 6 O 19 5Al 2 O 3 + 2BaCO 3 + 6Fe 2 O 3 + 2NiO + 0.5O 2 -->2BaNiAl 5 Fe 6 O 19 +2CO 2 BaNi 2 Al 4 Fe 6 O 19 4Al 2 O 3 + 2BaCO 3 + 6Fe 2 O 3 + 4NiO + O 2 -->2BaNi 2 Al 4 Fe 6 O 19 + 2CO 2 BaNi 3 Al 3 Fe 6 O 19 3Al 2 O 3 + 2BaCO 3 + 6Fe 2 O 3 + 6NiO + 1.5O 2 -->2BaNi 3 Al 3 Fe 6 O 19 +2CO 2 BaAl 6 Fe 6 O 19 0.010657 BaNi 0.5 Al 5.5 Fe 6 O 19 0.01048 BaNiAl 5 Fe 6 O 19 0.010309 BaNi 2 Al 4 Fe 6 O 19 0.009982 BaNi 3 Al 3 Fe 6 O 19 0.009676

Massa : 10 gram Elemen Ar Al 26.98 Ba 137.33 Ca 40.08 Sr 87.62 Fe 55.85 C 12.01 O 16.00 Ni 58.71 Oksida Mr Massa (gr) Massa (gr) Massa (gr) Massa (gr) Massa (gr) Al 2 O 3 101.96 3.2600 2.9386 2.6278 2.0356 1.4799 BaCO 3 197.34 2.1031 2.0682 2.0343 1.9699 1.9094 NiO 74.71 0.3915 0.7702 1.4916 2.1686 Fe 2 O 3 159.70 5.1059 5.0210 4.9389 4.7825 4.6357 BaAl 6 Fe 6 O 19 938.3192 10.0000 BaNi 0.5 Al 5.5 Fe 6 O 19 954.1835 10.0000 BaNi Al 5 Fe 6 O 19 970.0477 10.0000 BaNi 2 Al 4 Fe 6 O 19 1001.776 10.0000 BaNi 3 Al 3 Fe 6 O 19 1033.505 10.0000 O 2 32 0.0419 0.0825 0.1597 0.2322 CO 2 44.01 0.4690 0.4612 0.4537 0.4393 0.4258 Total 10.4690 10.4612 10.4537 10.4393 10.4258

Massa Sebelum Total Massa Sesudah 10.4690 10.4612 10.4537 10.4393 10.4258 LAMPIRAN C Hasil XRD Menggunakan MATCH Sampel BaNi x Al 6-x Fe 6 O 19 BaAl 6 Fe 6 O 19

Puncak-Puncak Difraksi Sinar-X BaAl 6 Fe 6 O 19 No. Sudut Intensitas Bidang (hkl) Fasa h K L 1. 17.985 784.28 1 0 1 Barium Heksaferit 2. 23.2751 1511.63 1 0 4 Barium Heksaferit 3. 30.6663 4548.18 1 1 0 Barium Heksaferit 4. 31.166 3600.8 1 1 2 Barium Heksaferit 5. 31.7034 2025.03 1 1 2 Barium Heksaferit 6. 34.5055 7176.31 2 0 0 Barium Heksaferit 7. 35.6028 1412.47 1 0 8 Barium Heksaferit 8. 38.851 171.56 1 1 6 Barium Heksaferit 9. 39.7478 438.91 1 0 9 Barium Heksaferit 10. 40.8227 3221.54 1 0 10 Barium Heksaferit 11. 42.9328 1341.27 1 0 10 Barium Heksaferit 12. 46.4115 235.7 1 0 11 Barium Heksaferit 13. 47.2366 298.27 2 1 1 Barium Heksaferit 14. 50.8281 789.01 2 0 9 Barium Heksaferit 15. 54.5238 335.5 3 0 2 Barium Heksaferit 16. 55.7378 2424.83 0 0 14 Barium Heksaferit 17. 57.2651 3076.75 2 1 8 Barium Heksaferit

18. 59.1339 239.07 2 1 9 Barium Heksaferit 19. 63.8881 2118.06 2 0 13 Barium Heksaferit 20. 65.601 431.9 2 1 11 Barium Heksaferit 21. 68.3032 547.86 3 0 10 Barium Heksaferit 22. 75.166 142.88 4 0 3 Barium Heksaferit 23. 76.5383 170.17 1 0 18 Barium Heksaferit 24. 78.1809 153.12 4 0 6 Barium Heksaferit BaAl 0,5 Al 5,5 Fe 6 O 19 Puncak-Puncak Difraksi Sinar-X BaNi 0,5 Al 5,5 Fe 6 O 19 No. Sudut Intensitas Bidang (hkl) Fasa h K l 1. 17.8679 305.83 1 0 1 Barium Heksaferit 2. 23.1416 657 1 0 4 Barium Heksaferit 3. 23.988 216.04 1 0 4 Barium Heksaferit 4. 28.2914 266.38 1 0 6 Barium Heksaferit 5. 30.5601 2344.39 1 1 0 Barium Heksaferit 6. 31.0194 893.38 1 1 2 Barium Heksaferit 7. 31.5733 807.41 1 1 2 Barium Heksaferit 8. 34.374 4047.63 1 1 4 Barium Heksaferit 9. 35.4618 534.29 2 0 1 Barium Heksaferit 10. 40.6525 1478.38 2 0 5 Barium Heksaferit 11. 42.7717 827.54 1 0 10 Barium Heksaferit 12. 46.9096 229.89 1 0 11 Barium Heksaferit 13. 50.6879 409.27 2 0 9 Barium Heksaferit

14. 54.3688 207.2 3 0 2 Barium Heksaferit 15. 55.5478 1457.31 0 0 14 Barium Heksaferit 16. 57.0196 1657.42 2 1 8 Barium Heksaferit 17. 63.6781 1297.41 2 0 13 Barium Heksaferit 18. 67.9666 271.43 4 0 0 Barium Heksaferit 19. 68.8769 168.34 3 0 10 Barium Heksaferit 20. 72.5375 181.08 3 1 7 Barium Heksaferit 21. 76.3047 171.99 1 0 18 Barium Heksaferit 22. 78.3469 90.75 4 0 6 Barium Heksaferit BaNiAl 5 Fe 6 O 19 Puncak-Puncak Difraksi Sinar-X BaNiAl 5 Fe 6 O 19 No. Sudut Intensitas Bidang (hkl) Fasa h K 1 1. 17.8364 311.44 1 0 1 Barium Heksaferit 2. 23.0229 540.31 1 0 4 Barium Heksaferit 3. 30.5072 1881.55 1 1 0 Barium Heksaferit 4. 31.4959 650.64 1 1 2 Barium Heksaferit 5. 34.3123 3368.61 1 1 4 Barium Heksaferit 6. 35.4365 458.73 2 0 1 Barium Heksaferit 7. 40.5818 1159.9 2 0 5 Barium Heksaferit 8. 42.717 694.73 1 0 10 Barium Heksaferit 9. 46.8052 137.9 1 0 11 Barium Heksaferit 10. 50.5276 341.95 2 0 9 Barium Heksaferit 11. 54.3393 145.31 3 0 2 Barium Heksaferit 12. 55.4834 1211.11 0 0 14 Barium Heksaferit

13. 56.9289 1557.34 1 1 12 Barium Heksaferit 14. 63.6423 1263.6 2 0 13 Barium Heksaferit 15. 64.9934 168.55 1 1 14 Barium Heksaferit 16. 67.8417 273.97 2 0 14 Barium Heksaferit 17. 76.2965 130.38 1 0 18 Barium Heksaferit BaNi 2 Al 4 Fe 6 O 19 Data Puncak-Puncak Difraksi Sinar-X BaNi 2 Al 4 Fe 6 O 19 No. Sudut Intensitas Bidang (hkl) Fasa H K 1 1. 17.8153 336.92 1 0 1 Barium Heksaferit 2. 22.9747 314.71 0 0 6 Barium Heksaferit 3. 28.1768 845.3 1 0 6 Barium Heksaferit 4. 30.4389 2516.18 1 1 0 Barium Heksaferit 5. 31.4313 620.44 1 1 2 Barium Heksaferit 6. 32.2217 3038.47 1 0 7 Barium Heksaferit 7. 34.2299 3815.77 1 1 4 Barium Heksaferit 8. 35.8171 1585.22 3 1 1 Nikel Ferit 9. 36.654 157.77 2 0 2 Barium Heksaferit 10. 37.2393 1732.73 2 2 2 Nikel Ferit 11. 40.492 999.83 2 0 5 Barium Heksaferit

12. 42.5903 644.63 2 0 6 Barium Heksaferit 13. 46.598 210.05 1 0 11 Barium Heksaferit 14. 50.4074 362.44 2 0 9 Barium Heksaferit 15. 53.4902 174.05 2 0 10 Barium Heksaferit 16. 54.2087 384.76 3 0 2 Barium Heksaferit 17. 55.3701 1170.91 0 0 14 Barium Heksaferit 18. 56.765 1503.72 1 1 12 Barium Heksaferit 19. 57.7031 748.82 2 2 2 Barium Oksida 20. 63.5207 1867.32 2 0 13 Barium Heksaferit 21. 66.0687 87.7 5 3 1 Nikel Ferit 22. 67.6887 212.27 4 0 0 Barium Oksida 23. 76.1897 174.91 1 0 18 Barium Heksaferit BaNi 3 Al 3 Fe 6 O 19 Data puncak-puncak Difraksi Sinar-X Sampel BaNi 3 Al 3 Fe 6 O 19 No. Sudut Intensitas Bidang (hkl) Fasa h K l 1. 18.3881 282.36 1 0 2 Barium Heksaferit 2. 22.3433 336.36 0 0 6 Barium Heksaferit 3. 28.5156 1093.64 1 0 6 Barium Heksaferit 4. 30.6966 2239.41 0 0 8 Barium Heksaferit 5. 31.8085 2064.09 1 1 2 Barium Heksaferit 6. 32.4668 1387.77 2 0 0 Barium Oksida 7. 34.5167 2077.08 1 1 4 Barium Heksaferit

8. 36.086 3845.36 2 0 2 Barium Heksaferit 9. 37.5097 1459.76 2 2 2 Nikel Ferit 10. 40.6822 371.3 2 0 5 Barium Heksaferit 11. 42.8526 397.44 1 0 10 Barium Heksaferit 12. 43.555 1175.64 4 0 0 Nikel Ferit 13. 54.481 390.94 3 0 2 Barium Heksaferit 14. 55.6257 522.23 0 0 14 Barium Heksaferit 15. 57.0303 750.91 2 1 8 Barium Heksaferit 16. 57.9773 1099.04 2 2 2 Barium Oksida 17. 63.7311 2090.03 2 0 13 Barium Heksaferit 18. 64.7572 515.61 1 1 14 Barium Heksaferit 19. 66.2065 301.31 5 3 1 Nikel Ferit 20. 67.6861 111.39 4 0 0 Barium Oksida 21. 75.4058 389.26 4 0 3 Barium Heksaferit 22. 77.9069 452.01 4 0 5 Barium Heksaferit LAMPIRAN D Hasil SEM/EDS Sampel BaNiAl 5 Fe 6 O 19

Komposisi Sampel BaNiAl 5 Fe 6 O 19 No. Elemen Kimia % Berat % Atom 1. Carbon C 9.47 18.73 2. Oksigen O 41.76 62.01 3. Natrium Na 0.34 0.35 4. Magnesium Mg 0.55 0.54 5. Alumunium Al 5.72 5.04 6. Silikon Si 0.26 0.22 7. Titanium Ti 2.95 1.46 8. Besi Fe 14.01 5.96

9. Nikel Ni 5.91 2.39 10. Barium Ba 19.01 3.29 LAMPIRAN E Hasil VSM Kurva HIsterisis Sampel BaNi x Al 6-x Fe 6 O 19 BaAl 6 Fe 6 O 19 BaNi 0,5 Al 5,5 Fe 6 O 19

BaNiAl 5 Fe 6 O 19 BaNi 2 Al 4 Fe 6 O 19 LAMPIRAN F BaNi 3 Al 3 Fe 6 O 19 Hasil VNA Sampel BaNi x Al 6-x Fe 6 O 19

BaAl6Fe6O19

BaNi 0,5 Al 5,5 Fe 6 O 19 BaNiAl 5 Fe 6 O 19

BaNi 2 Al 4 Fe 6 O 19 BaNi 3 Al 3 Fe 6 O 19