Lampiran 1 Hasil Penelitian Pendahuluan Hasil Uji Vitamin C dengan Pemanasan 1 C dalam Sawi Putih Waktu (menit) Vitamin C (mg/1gr) 6 -,4153 6,656 6,2536 6 -,3454 6 -,3585 6 -,341 35 4,131 35 3,897 35 2,7978 35 3,164 35 3,4842 35 2,1683 Hasil Uji Vitamin C dengan Pemanasan 7 C dalam Sawi Putih Waktu (menit) Vitamin C (mg/1gr) 6 1,754 6 2,53 6 1,1847 35 4,731 35 5,6918 35 5,1322 15 15,9169 15 16,949 15 16,661 Hasil Uji Vitamin C dalam Air Rebusan Waktu (menit) Vitamin C (mg/1gr) 6,6295 6,7213 6,4678 35 1,176 35 1,3727 35 1,579 15 1,7967 15 2,59 15 1,844 43
44 Lampiran 2 Hasil Observasi Nama (Rumah Makan) Bentuk Masakan Waktu yang Diperlukan Untuk Merebus Perlakuan Sebelum Direbus Tinah (Warteg Ferdi) Cap Cai Kuah 1-15 Menit - Dicuci - Dipotong Murni (Pentul) Cap Cai Kuah 12-15 Menit - Dicuci - Dipotong potong Asih (MM) Minah (Warteg 24 Jam) Bambang (Warteg Bambang) Cap Cai Kuah Sawi Rebus Telur 15 Menit - Dihilangkan Bagian yang rusak - Dicuci - Dipotong potong Cap Cai Kuah 15 menit - dicuci - dipotong Cap Cai Kuah 3 menit - Dihilangkan bagian yang rusak - dicuci - dipotong
45 Lampiran 3. Kurva Standar Vitamin C,8,7 y = -,183x +,7116 R 2 =,98,6,5,4,3,2,1, 4 8 12 16 2 24 28 32 36 4 44
46 Lampiran 4. Kurva Standar Fenol 1,2 1 y =,112x +,41 R 2 =,9892 absorbansi,8,6,4,2 2 4 6 8 1 Konsentrasi quercetin (ppm)
47 Lampiran 5 Hasil Pengujian SPSS Vitamin C, Fenol dan Aktivitas Antioksidan Vitamin C dalam Sawi Putih VitaminC waktu, 6, 12, 2, 25, 45, Tests of Normality Kolmogorov-Smirnov a Shapiro-Wilk Statistic df Sig. Statistic df Sig.,227 6,2*,9 6,374,17 6,2*,97 6,891,218 6,2*,945 6,7,215 6,2*,934 6,68,227 6,2*,876 6,251,211 6,2*,967 6,873,254 6,2*,95 6,43,255 6,2*,91 6,433,258 6,2*,853 6,166,232 6,2*,91 6,435,292 6,121,815 6,8 *. This is a lower bound of the true significance. a. Lilliefors Significance Correction Descriptives VitaminC, 6, 12, 2, 25, 45, 95% Confidence Interval for Mean N Mean Std. Deviation Std. Error Lower Bound Upper Bound Minimum Maximum 6 28,69,31925,1333 28,3549 29,25 28,15 2 6 24,7745,65586,26775 24,862 25,4628 23,8 25,62 6 19,722 1,84548,75341 17,7835 21,6569 17,58 22,45 6 18,2718 1,3457,54938 16,8595 19,684 16,47 19,96 6 16,5261 1,2871,41997 15,4465 17,656 15,63 18,27 6 15,1556 2,41423,9856 12,622 17,6891 11,28 18,3 6 12,2951 2,5146 1,2636 9,6567 14,9334 7,9 15,51 6 8,4328 5,2675 2,1545 2,949 13,967 1,46 14,39 6 8,441 3,5541 1,24737 5,2336 11,6465 5,13 11,92 6 4,465 3,82166 1,5619,4499 8,4711,71 1,48 6 5,463 3,8482 1,55331 1,471 9,4559 2,24 1,61 66 14,7481 7,94622,97811 12,7947 16,716,71 2 ANOVA VitaminC Between Groups Within Groups Sum of Squares df Mean Square F Sig. 3678,654 1 367,865 47,539, 425,599 55 7,738 414,253 65
48 Duncan a waktu 45, 25, 2, 12, 6,, Sig. VitaminC Subset for alpha =.5 N 1 2 3 4 5 6 7 6 4,465 6 5,463 5,463 6 8,4328 6 8,441 6 12,2951 6 15,1556 15,1556 6 16,5261 16,5261 6 18,2718 18,2718 6 19,722 6 24,7745 6 28,69,535,85,8,71,64 1, 1, Means for groups in homogeneous subsets are displayed. a. Uses Harmonic Mean Sample Size = 6,. Vitamin C dalam Air Rebusan vitaminc waktu Tests of Normality Kolmogorov-Smirnov a Shapiro-Wilk Statistic df Sig. Statistic df Sig.,19 6,2*,913 6,454,243 6,2*,851 6,16,292 6,12,883 6,281,213 6,2*,919 6,495,287 6,133,92 6,54 *. This is a lower bound of the true significance. a. Lilliefors Significance Correction Descriptives vitaminc 95% Confidence Interval for Mean N Mean Std. Deviation Std. Error Lower Bound Upper Bound Minimum Maximum 6 2,437,291,11843 2,992 2,781 2,6 2,75 6 3,944,46347,18921 2,68 3,587 2,7 3,94 6 2,957,6477,26417 2,2266 3,5847 2,2 4,9 6 1,6779,1876,7659 1,4811 1,8748 1,46 1,93 6,7593,1858,7556,565,9535,52 1,6 3 2,1682,94742,17297 1,8144 2,5219,52 4,9 ANOVA vitaminc Between Groups Within Groups Sum of Squares df Mean Square F Sig. 22,95 4 5,524 35,88, 3,936 25,157 26,3 29
49 Duncan a waktu Sig. vitaminc Subset for alpha =.5 N 1 2 3 4 6,7593 6 1,6779 6 2,437 6 2,957 6 3,944 1, 1, 1,,418 Means for groups in homogeneous subsets are displayed. a. Uses Harmonic Mean Sample Size = 6,. Aktivitas Antioksidan dalam Sawi Putih antioksidan waktu, 6, 12, 2, 25, 45, Tests of Normality Kolmogorov-Smirnov a Shapiro-Wilk Statistic df Sig. Statistic df Sig.,245 6,2*,891 6,323,37 6,8,772 6,32,164 6,2*,98 6,951,232 6,2*,93 6,39,271 6,192,865 6,26,216 6,2*,932 6,596,186 6,2*,928 6,563,17 6,2*,955 6,78,216 6,2*,955 6,777,188 6,2*,957 6,799,246 6,2*,922 6,52 *. This is a lower bound of the true significance. a. Lilliefors Significance Correction Descriptives VitaminC, 6, 12, 2, 25, 45, 95% Confidence Interval for Mean N Mean Std. Deviation Std. Error Lower Bound Upper Bound Minimum Maximum 6 45,56 2,84513 1,16152 42,5148 48,4863 42,61 5,7 6 41,6891 12,94276 5,28386 28,165 55,2717 29,4 55,8 6 37,824 2,14753,87673 35,5487 4,561 35,12 41,7 6 34,2947 4,7993 1,95919 29,2584 39,331 26,16 39,2 6 32,3755 3,22757 1,31765 28,9884 35,7626 28,87 36,26 6 27,7116 3,6425 1,47143 23,9292 31,494 21,42 31,71 6 27,437 7,29166 2,97681 19,7516 35,559 18,38 36,26 6 19,4924 1,92485,78582 17,4724 21,5124 16,89 21,88 6 1,3111 1,43852,58727 8,815 11,828 7,9 12,14 6 3,9562 2,83128 1,15587,985 6,9275,4 7,83 6 5,7194 1,23745,5519 4,428 7,181 4,3 7,39 66 26,233 14,6791 1,79811 22,4323 29,6144,4 55,8
5 ANOVA antioksidan Between Groups Within Groups Sum of Squares df Mean Square F Sig. 12394,675 1 1239,467 46,194, 1475,752 55 26,832 1387,427 65 Duncan a waktu 45, 25, 2, 12, 6,, Sig. antioksidan Subset for alpha =.5 N 1 2 3 4 5 6 7 6 3,9562 6 5,7194 5,7194 6 1,3111 6 19,4924 6 27,437 6 27,7116 6 32,3755 32,3755 6 34,2947 6 37,824 37,824 6 41,6891 41,6891 6 45,56,558,13 1,,122,91,199,28 Means for groups in homogeneous subsets are displayed. a. Uses Harmonic Mean Sample Size = 6,. Aktivitas Antioksidan Air Rebusan Tests of Normality Kolmogorov-Smirnov a Shapiro-Wilk waktu Statistic df Sig. Statistic df Sig. antioksidan,186 6,2*,958 6,84,149 6,2*,97 6,893,191 6,2*,976 6,93,152 6,2*,986 6,977,193 6,2*,934 6,68 *. This is a lower bound of the true significance. a. Lilliefors Significance Correction Descriptives antioksidan 95% Confidence Interval for Mean N Mean Std. Deviation Std. Error Lower Bound Upper Bound Minimum Maximum 6 4,861 1,35878,55472 3,381 6,232 3,21 7,1 6 9,5656 1,89547,77382 7,5765 11,5548 7,31 12,62 6 6,2513 1,12152,45786 5,743 7,4282 4,7 7,83 6 2,6313 1,22416,49976 1,3466 3,916 1,6 4,51 6,8751,98684,4287 -,165 1,917 -,19 2,58 3 4,8259 3,29775,628 3,5945 6,573 -,19 12,62
51 ANOVA antioksidan Between Groups Within Groups Sum of Squares df Mean Square F Sig. 269,533 4 67,383 36,744, 45,846 25 1,834 315,379 29 Duncan a waktu Sig. antioksidan Subset for alpha =.5 N 1 2 3 4 6,8751 6 2,6313 6 4,861 6 6,2513 6 9,5656 1, 1,,76 1, Means for groups in homogeneous subsets are displayed. a. Uses Harmonic Mean Sample Size = 6,. Fenol Dalam Sawi Putih Descriptives Fenol, 6, 12, 2, 25, 45, 95% Confidence Interval for Mean N Mean Std. Deviation Std. Error Lower Bound Upper Bound Minimum Maximum 6 1212,2917 185,24661 75,62661 117,8873 146,6961 87,57 136,86 6 758,2798 65,3675 26,55114 69,279 826,5316 667,7 839,54 6 56,869 97,72488 39,8961 458,3131 663,425 485,18 737,79 6 696,283 15,65965 61,5654 538,17 854,3159 516,61 853,29 6 435,744 18,1456 7,39116 416,7445 454,7436 47,39 457,29 6 473,5893 17,22265 7,3112 455,5152 491,6634 449,82 498,93 6 491,5952 28,43338 11,6788 461,7562 521,4342 437,25 513,7 6 446,2857 6,548 24,71568 382,752 59,8194 382,64 521,32 6 319,722 2,29276 8,28448 298,4243 341,162 3,14 357,89 6 316,6429 7,1411 28,63495 243,344 39,2513 241,21 395,21 6 338,5119 5,1915 2,496 285,8392 391,1847 268,71 386,18 66 549,9762 264,6154 32,5719 484,9256 615,268 241,21 136,86
52 Fenol Waktu, 6, 12, 2, 25, 45, Tests of Normality Kolmogorov-Smirnov a Shapiro-Wilk Statistic df Sig. Statistic df Sig.,211 6,2*,836 6,122,162 6,2*,97 6,895,295 6,111,818 6,84,279 6,158,839 6,129,227 6,2*,944 6,694,126 6,2*,994 6,997,279 6,158,785 6,43,218 6,2*,861 6,192,255 6,2*,849 6,154,242 6,2*,843 6,137,279 6,157,866 6,29 *. This is a lower bound of the true significance. a. Lilliefors Significance Correction ANOVA Fenol Between Groups Within Groups Sum of Squares df Mean Square F Sig. 4132668 1 413266,828 54,284, 418716,7 55 7613,32 4551385 65 Duncan a Waktu 45, 12, 25, 2, 6,, Sig. Fenol Subset for alpha =.5 N 1 2 3 4 5 6 6 316,6429 6 319,722 6 338,5119 338,5119 6 435,744 435,744 6 446,2857 6 473,5893 473,5893 6 491,5952 491,5952 6 56,869 6 696,283 6 758,2798 6 1212,2917,686,59,32,17,223 1, Means for groups in homogeneous subsets are displayed. a. Uses Harmonic Mean Sample Size = 6,. Fenol dalam Air Rebusan
53 Descriptives Fenol 95% Confidence Interval for Mean N Mean Std. Deviation Std. Error Lower Bound Upper Bound Minimum Maximum 6 26,595 14,26816 5,82495 11,86 41,33 2,75 42,4 6 3 19,93145 8,13698 12,832 53,9168 3,93 64,43 6 39,5476 8,8433 3,342 31,636 48,316 3,25 51,46 6 151,5774 26,7217 1,999 123,5347 179,621 124,14 193,29 6 193,5476 64,35363 26,27226 126,126 261,826 131,61 259,29 3 88,7464 77,4466 14,13975 59,8274 117,6655 2,75 259,29 ANOVA Fenol Between Groups Within Groups Sum of Squares df Mean Square F Sig. 146333,1 4 36583,28 33,127, 2768,192 25 114,328 173941,3 29 Duncan a Waktu Sig. Fenol Subset for alpha =.5 N 1 2 3 6 26,595 6 3 6 39,5476 6 151,5774 6 193,5476,514 1, 1, Means for groups in homogeneous subsets are displayed. a. Uses Harmonic Mean Sample Size = 6,. Fenol Waktu Tests of Normality Kolmogorov-Smirnov a Shapiro-Wilk Statistic df Sig. Statistic df Sig.,229 6,2*,933 6,67,18 6,2*,976 6,928,164 6,2*,956 6,787,259 6,2*,895 6,347,294 6,113,751 6,21 *. This is a lower bound of the true significance. a. Lilliefors Significance Correction Kadar Air
54 KadarAir Waktu, 6, 12, 2, 25, 45, Tests of Normality Kolmogorov-Smirnov a Shapiro-Wilk Statistic df Sig. Statistic df Sig.,192 6,2*,925 6,541,235 6,2*,959 6,813,38 6,79,836 6,122,174 6,2*,913 6,455,238 6,2*,944 6,694,27 6,197,883 6,282,291 6,122,86 6,67,238 6,2*,94 6,663,34 6,88,83 6,18,289 6,129,86 6,188,184 6,2*,952 6,756 *. This is a lower bound of the true significance. a. Lilliefors Significance Correction Descriptives KadarAir, 6, 12, 2, 25, 45, 95% Confidence Interval for Mean N Mean Std. Deviation Std. Error Lower Bound Upper Bound Minimum Maximum 6,9568,536,219,9511,9624,95,96 6,9557,1243,58,9426,9687,94,97 6,9479,156,615,9321,9637,92,96 6,9572,63,246,959,9635,95,96 6,9519,727,297,9443,9596,94,96 6,9598,496,22,9546,965,95,97 6,9578,829,339,9491,9665,95,96 6,9542,119,486,9417,9667,94,97 6,9534,1389,567,9389,968,93,96 6,954,1441,588,9352,9655,93,96 6,961,444,181,9564,9657,96,97 66,9551,117,125,9526,9576,92,97 ANOVA KadarAir Between Groups Within Groups Sum of Squares df Mean Square F Sig.,1 1,,911,53,6 55,,7 65
55 Duncan a Waktu 6, 45, 12, 25,, 2, Sig. KadarAir Subset for alpha =.5 N 1 6,9479 6,954 6,9519 6,9534 6,9542 6,9557 6,9568 6,9572 6,9578 6,9598 6,961,68 Means for groups in homogeneous subsets are displayed. a. Uses Harmonic Mean Sample Size = 6,.
56 Lampiran 6 Grafik Aktivitas Antioksidan, Fenol dan Vitamin C Aktivitas Antioksidan Batch 1 Aktivitas Antioksidan Sawi Putih 1 6 5 4 3 2 1 1 2 3 4 5 6 7 Aktivitas Antioksidan Air Rebusan 1 14 12 1 8 6 4 2-2 1 2 3 4 5 6 7 Aktivitas Antioksidan Batch 2 Aktivitas Antioksidan Sawi Putih 2 5 45 4 35 3 25 2 15 1 5 1 2 3 4 5 6 7 Aktivitas Antioksidan Air Rebusan 2 12 1 8 6 4 2 1 2 3 4 5 6 7 Fenol Batch 1 Fenol Sawi Putih 1 16 14 12 1 8 6 4 2 1 2 3 4 5 6 7 Fenol Air Rebusan 1 3 25 2 15 1 5 1 2 3 4 5 6 7 Fenol Batch 2 Fenol Sawi Putih 2 16 14 12 1 8 6 4 2 1 2 3 4 5 6 7 Fenol Air Rebusan 2 16 14 12 1 8 6 4 2 1 2 3 4 5 6 7
57 Vitamin C Batch 1 Vitamin C Sawi Putih 1 35 3 25 2 15 1 5 1 2 3 4 5 6 7 Vitamin C Air Rebusan 1 5 4 4 3 3 2 2 1 1 1 2 3 4 5 6 7 Vitamin C Batch 2 Vitamin C Sawi Putih 2 35 3 25 2 15 1 5 1 2 3 4 5 6 7 Vitamin C Air Rebusan 2 4 3 3 2 2 1 1 1 2 3 4 5 6 7 Kadar Air
58 Kadar Air 1 1% Kadar air (%) 95% 9% 85% 8% 75% 1 2 3 4 5 6 7 Waktu (menit) Kadar Air 2 1% Kadar Air(%) 95% 9% 85% 8% 75% 1 2 3 4 5 6 7 Waktu (menit)