LAMPIRAN A. HASIL STANDARISASI SPESIFIK EKSTRAK TEH (Camellia sinensis Linn.) 1 5,40 2 5,42 3 5,42 x ± SD 5,41 ± 0,01.

LAMPIRAN A HASIL STANDARISASI SPESIFIK EKSTRAK TEH (Camellia sinensis Linn.) 1. Hasil Perhitungan ph Replikasi ph 1 5,40 2 5,42 3 5,42 x ± SD 5,41 ± 0,01 2. Hasil Perhitungan Kadar Sari Larut Air Replikasi Berat cawan (g) Berat ekstrak (g) Berat cawan + ekstrak setelah pemanasan (g) % Kadar sari larut air (%) 1 60,2735 5,0013 61,1789 90,52 2 58,4788 5,0009 59,3302 85,12 3 56,3903 5,0002 57,2525 86,22 x ± SD 87,29 ± 2,85 1. 93

2. 3. 3. Hasil Perhitungan Kadar Sari larut etanol Replikas i Berat cawan (g) Berat ekstrak (g) Berat cawan + ekstrak setelah pemanasan (g) % Kadar sari larut etanol (%) 1 55,3293 5,0002 55,9904 66,11 2 56,5430 5,0009 57,2156 67,25 3 44,3305 5,0012 45,0146 68,39 x ± SD 67,25 ± 1,14 1. 2. 3. 94

LAMPIRAN B HASIL STANDARISASI NON SPESIFIK EKSTRAK TEH (Camellia sinensis Linn.) 1. Hasil Perhitungan Susut Pengeringan Replikasi Susut Pengeringan 1 5,8 2 5,6 3 5,8 x ± SD 5,74 ± 0,12 2. Hasil Perhitungan Kadar Air Replikasi Berat cawan (g) Berat ekstrak (g) Berat cawan + ekstrak (g) % Kadar air (%) 1 36,1 10 45,7 4 2 56,8 10,1 66,4 4,95 3 42,7 10,1 52,3 4,95 x ± SD 4,63 ± 0,55 1. 95

2. 3. 3. Hasil Perhitungan Kadar Abu Total Replikasi Berat krus (g) Berat ekstrak (g) Berat krus + abu (g) % Kadar abu total (%) 1 27,8884 2,0003 28,0608 8,62 2 29,3086 2,0041 29,4840 8,75 3 28,6834 2,0079 28,8493 8,28 x ± SD 8,55 ± 0,24 1. Kadar AbuTotal x 100% 2. Kadar Abu Total x 100% 96

3. Kadar Abu x 100% 4. Hasil Perhitungan Kadar Abu Tidak Larut Asam Replikasi Berat krus (g) Berat ekstrak (g) Berat krus + abu + HCl (g) % Kadar Abu 1 29,2472 2,0010 29,2580 0,54 2 28,6605 2,0014 28,6721 0,58 3 25,0903 2,0001 25,0989 0,43 x ± SD 0,52 ± 0,08 1. 2. 3. 97

5. Hasil Perhitungan Kadar Abu Larut Air Replikasi Berat krus (g) Berat ekstrak (g) Berat krus + abu + air (g) % Kadar Abu 1 27,8884 2,0003 27,9440 2,78 2 29,3086 2,0041 29,3699 3,06 3 28,6834 2,0079 28,7439 3,01 x ± SD 2,95 ± 0,15 1. 2. 3. 98

LAMPIRAN C CONTOH PERHITUNGAN H HITUNG Keterangan: 1 Perhitungan peringkat : n x n 1 dimana : n adalah jumlah pengamatan yang dilakukan Kruskal-wallis (H) : 12 H = xssak 3 N N ( N + 1) ( + 1) dimana : N adalah jumlah total pengamatan dalam penelitian (contoh. N = 9, dan setiap kelompok diamati 3 kali) SSak : jumlah kuadrat antar kelompok Perhitungan: Peringkat : SSak : H hitung : 99

LAMPIRAN D HASIL UJI HOMOGENITAS SEDIAAN Kriteria Penilaian pada Parameter Homogenitas Hand Body Lotion Kriteria Penilaian Skor Keterangan Tidak homogen - Kurang homogen + Homogen ++ 0 1 2 Ada butiran kasar dan sediaan memisah Ada butiran kasar dan sediaan tidak memisah Tidak ada butiran kasar dan sediaan tidak memisah Hasil Pengamatan Homogenitas Hand Body Lotion Replikasi Formula I Formula II Formula III Bets 1 Bets 2 Bets 1 Bets 2 Bets 1 Bets 2 1 ++ + + + ++ ++ 2 ++ + + + ++ ++ 3 ++ + + + ++ ++ 100

LAMPIRAN E HASIL UJI DAYA SEBAR SEDIAAN Kriteria Penilaian Uji Daya Sebar Hand Body Lotion Kriteria Penilaian Skor Keterangan Buruk - 0 Jika diameter penyebaran < 4 cm Baik + 1 Jika diameter penyebaran 4-6 cm Sangat baik ++ 2 Jika diameter penyebaran > 6 cm Hasil Pengamatan Daya Sebar Sediaan dengan Beban 125 gram Formula Rep Bets 1 Bets 2 Rata2 Pertambahan Awal Akhir Awal Akhir Awal Akhir diameter Skor I II III 1 2,00 6,20 2,20 5,70 2,10 5,95 3,85 0 2 1,80 5,70 2,20 6,10 2,00 5,90 3,90 0 3 2,00 5,90 2,10 6,10 2,05 6,00 3,95 0 3,90 ± 0,05 1 2,40 6,40 2,20 6,30 2,30 6,35 4,05 0 2 2,50 6,50 2,20 6,40 2,35 6,45 4,10 0 3 2,60 6,60 2,10 6,20 2,35 6,4 4,05 0 4,07 ± 0,03 1 2,40 6,40 2,20 5,90 2,30 6,15 3,85 0 2 2,30 6,20 2,30 6,30 2,30 6,25 3,95 0 3 2,40 6,50 2,20 6,20 2,30 6,35 4,05 0 3,95 ± 0,10 101

LAMPIRAN F HASIL UJI VISKOSITAS SEDIAAN Formula Bets Nomor spindle Replikasi % Viskositas (cps) I 1 3 (5,0 RPM) 1 87,1 21140 2 84,8 20440 3 82,2 19800 20460 ± 670,22 2 3 (5,0 RPM) 1 82,1 19700 2 82,2 19820 3 81,7 19720 19746,67 ± 64,29 II 1 2 (1,5 RPM) 1 88,1 17820 2 87,8 17540 3 88,2 17800 17720 ± 156,20 2 2 (1,5 RPM) 1 89,2 18060 2 88,9 18020 3 88,7 17740 17940 ± 174,36 III 1 2 (1,0 RPM) 1 61,8 19100 2 60,1 19000 3 60,8 18900 19000 ± 100,00 2 2 (1,0 RPM) 1 65,1 19510 2 64,7 19470 3 64,2 19617 19532,33 ±76,00 102

LAMPIRAN G HASIL UJI PH SEDIAAN Formula Replikasi Bets 1 Bets 2 1 5,66 5,60 I 2 5,63 5,62 3 5,65 5,61 5,65 ± 0,02 5,61 ±0,01 1 5,47 5,52 II 2 5,45 5,49 3 5,48 5,46 5,47 ± 0,02 5,49 ± 0,03 1 5,49 5,50 III 2 5,50 5,45 3 5,51 5,48 5,50 ± 0,01 5,48 ± 0,03 103

LAMPIRAN H CONTOH PERHITUNGAN PERSENTASE PENGURANGAN PENGUAPAN AIR a. Pertambahan berat Pertambahan berat Berat silika awal Berat silika akhir Pertambahan berat = berat silika akhir berat silika awal = 10,0053 g = 10,1128 g = 0,1075 g b. Persentase pengurangan penguapan 100% Pertambahan berat tanpa sediaan Pertambahan berat sediaan = 0,1075 g = 0,0897 g Persentase pengurangan penguapan = 16,56% 104

LAMPIRAN I HASIL UJI EFEKTIFITAS Formula Bets Replikasi Berat silica Pertambaha % pengurangan Awal (g) Akhir (g) n berat penguapan Blangko 1 9,9639 10,0677 0,1038 2 9,9846 10,0860 0,1014 3 10,0674 10,1847 0,1173 10,0053 10,1128 0,1075 0,00% Basis 1 10,0427 10,1324 0,0897 16,56% 2 10,0110 10,1021 0,0911 15,26% 3 10,0334 10,1299 0,0965 10,23% 14,02% Formula I Formula II Formula III 1 1 9,9671 10,0307 0,0636 40,84% 2 10,0423 10,1208 0,0785 26,98% 3 10,0104 10,0696 0,0592 44,93% 37,58% 2 1 10,0303 10,1096 0,0793 26,23% 2 10,0462 10,1088 0,0626 41,76% 3 10,0454 10,0844 0,0668 37,86% 35,28% 1 1 10,0007 10,0864 0,0857 20,28% 2 9,9912 10,0743 0,0831 22,69% 3 10,0575 10,1462 0,0887 17,49% 20,15% 2 1 10,0295 10,1076 0,0817 24,00% 2 10,0462 10,1297 0,0835 22,33% 3 10,0315 10,1142 0,0827 23,07% 23,13% 1 1 10,0190 10,0953 0,0763 29,02% 2 10,0042 10,0786 0,0744 30,79% 3 10,0454 10,1161 0,0707 34,23% 31,35% 2 1 9,9706 10,0387 0,0681 36,65% 2 10,0509 10,1228 0,0719 33,12% 3 9,9104 9,9829 0,0725 32,56% 34,11% 105

LAMPIRAN J HASIL UJI STATISTIK PH ANTAR BETS DAN ANTAR FORMULA SEDIAAN ANTAR BETS: t-test FORMULA I Paired Samples Statistics Mean N Std. Deviation Std. Error Mean Pair 1 bets1 5.6467 3.01528.00882 bets2 5.6100 3.01000.00577 Paired Samples Correlations N Correlation Sig. Pair 1 bets1 & bets2 3 -.982.121 Paired Samples Test Mean Paired Differences t df Sig. (2- Std. Std. 95% Confidence tailed) Deviation Error Interval of the Mean Difference Pair 1 bets1 - bets2 Lower Upper.03667.02517.01453 -.02585.09918 2.524 2.128 107

FORMULA II Paired Samples Statistics Mean N Std. Deviation Std. Error Mean Pair 1 bets1 5.4667 3.01528.00882 bets2 5.4900 3.03000.01732 Paired Samples Correlations N Correlation Sig. Pair 1 bets1 & bets2 3 -.327.788 Pai r 1 bets1 - bets2 Mean Std. Deviation Paired Samples Test Paired Differences t Df Sig. (2- tailed) Std. Error Mean 95% Confidence Interval of the Difference Lower Upper -.02333.03786.02186 -.11738.07071-1.067 2.398 FORMULA III Paired Samples Statistics Mean N Std. Deviation Std. Error Mean Pair 1 bets1 5.5000 3.01000.00577 bets2 5.4767 3.02517.01453 108

Paired Samples Correlations N Correlation Sig. Pair 1 bets1 & bets2 3 -.397.740 Paired Samples Test Pair 1 bets1 - bets2 Mean Std. Deviation Paired Differences t Df Sig. (2- Std. Error tailed) Mean 95% Confidence Interval of the Difference Lower Upper.02333.03055.01764 -.05256.09922 1.323 2.317 ANTAR FORMULA Descriptives ph N Mean Std. Deviation Std. Error 95% Confidence Interval for Mean Lower Bound Upper Bound Minimum Maximum formula1 6 5.6283.02317.00946 5.6040 5.6526 5.60 5.66 formula2 6 5.4783.02483.01014 5.4523 5.5044 5.45 5.52 formula3 6 5.4883.02137.00872 5.4659 5.5108 5.45 5.51 Total 18 5.5317.07374.01738 5.4950 5.5683 5.45 5.66 Test of Homogeneity of Variances ph Levene Statistic df1 df2 Sig..090 2 15.914 109

ANOVA ph Sum of Squares df Mean Square F Sig. Between Groups.084 2.042 78.634.000 Within Groups.008 15.001 Total.092 17 Multiple Comparisons Dependent Variable: ph Tukey HSD (I) formula (J) formula Mean Difference (I-J) Std. Error Sig. 95% Confidence Interval Lower Bound Upper Bound formula1 formula2.15000 *.01337.000.1153.1847 formula3.14000 *.01337.000.1053.1747 formula2 formula1 -.15000 *.01337.000 -.1847 -.1153 formula3 -.01000.01337.740 -.0447.0247 formula3 formula1 -.14000 *.01337.000 -.1747 -.1053 formula2.01000.01337.740 -.0247.0447 *. The mean difference is significant at the 0.05 level. ph Tukey HSD formula N Subset for alpha = 0.05 formula2 6 5.4783 formula3 6 5.4883 1 2 formula1 6 5.6283 Sig..740 1.000 Means for groups in homogeneous subsets are displayed. a. Uses Harmonic Mean Sample Size = 6.000. 110

LAMPIRAN K HASIL UJI STATISTIK VISKOSITAS ANTAR BETS DAN ANTAR FORMULA SEDIAAN ANTAR BETS FORMULA I: Paired Samples Statistics Mean N Std. Deviation Std. Error Mean Pair 1 bets1 20460.0000 3 670.22384 386.95392 bets2 19746.6667 3 64.29101 37.11843 Paired Samples Correlations N Correlation Sig. Pair 1 bets1 & bets2 3 -.181.884 Pair 1 bets1 - bets2 Mean 713.3 3333 Paired Samples Test Paired Differences t df Sig. (2- Std. Std. 95% Confidence tailed) Deviation Error Interval of the Mean Difference Lower Upper 684.7870 7 395.362 00-987.772 06 2414.43 872 1.804 2.213 111

FORMULA II: Pair 1 Paired Samples Statistics Mean N Std. Deviation Std. Error Mean bets1 17720.0000 3 156.20499 90.18500 bets2 17940.0000 3 174.35596 100.66446 Paired Samples Correlations N Correlation Sig. Pair 1 bets1 & bets2 3 -.338.781 Paired Samples Test Pair 1 bets 1 - bets 2 Mean - 220.00000 Std. Deviation 270.5549 9 Paired Differences t df Sig. Std. Error Mean 156.2049 9 95% Confidence Interval of the Difference Lower Upper - 892.0958 4 452.09584-1.408 (2- tailed) 2.294 t hitung (-1,408) > t tabel (2.919), tidak terdapat perbedaan bermakna. 112

FORMULA III: Pair 1 Paired Samples Statistics Mean N Std. Deviation Std. Error Mean bets1 19000.0000 3 100.00000 57.73503 bets2 19532.3333 3 76.00219 43.87989 Paired Samples Correlations N Correlation Sig. Pair 1 bets1 & bets2 3 -.704.503 Paired Samples Test Pair 1 bets1 - bets2 Mean -532.33333 Std. Deviatio n 162.715 50 Paired Differences t df Sig. (2- tailed) Std. Error Mean 93.943 84 95% Confidence Interval of the Difference Lower Upper -936.54104-128.12563-5.667 2.030 113

ANTAR FORMULA Descriptives viskositas formula 1 formula 2 formula 3 Total N Mean Std. Deviation 6 6 6 1 8 20103.333 3 17830.000 0 19266.166 7 19066.500 0 577.91580 190.89264 302.19889 1033.8872 5 Std. Error 235.933 14 77.9315 9 123.372 18 243.689 56 95% Confidence Interval for Mean Lower Bound 19496.84 79 17629.67 05 18949.02 84 18552.36 00 Upper Bound 20709.8 188 18030.3 295 19583.3 049 19580.6 400 Minimum Maximum 19700.00 21140.00 17540.00 18060.00 18900.00 19617.00 17540.00 21140.00 Test of Homogeneity of Variances viskositas Levene Statistic df1 df2 Sig. 4.529 2 15.029 ANOVA viskositas Sum of Squares df Mean Square F Sig. Between Groups 15862934.333 2 7931467.167 51.531.000 Within Groups 2308754.167 15 153916.944 Total 18171688.500 17 114

Multiple Comparisons Dependent Variable: viskositas Tukey HSD (I) formula (J) formula Mean Difference (I- J) formula1 formula2 Std. Error Sig. 95% Confidence Interval Lower Bound Upper Bound formula2 2273.33333 * 226.50750.000 1684.9868 2861.6798 formula3 837.16667 * 226.50750.006 248.8202 1425.5132 formula1-2273.33333 * 226.50750.000-2861.6798-1684.9868 formula3-1436.16667 * 226.50750.000-2024.5132-847.8202 formula3 formula1-837.16667 * 226.50750.006-1425.5132-248.8202 formula2 1436.16667 * 226.50750.000 847.8202 2024.5132 *. The mean difference is significant at the 0.05 level. viskositas Tukey HSD formula N Subset for alpha = 0.05 1 2 3 formula2 6 17830.0000 formula3 6 19266.1667 formula1 6 20103.3333 Sig. 1.000 1.000 1.000 Means for groups in homogeneous subsets are displayed. a. Uses Harmonic Mean Sample Size = 6.000. 115

LAMPIRAN L HASIL UJI STATISTIK EFEKTIFITAS ANTAR BETS DAN ANTAR FORMULA SEDIAAN ANTAR BETS FORMULA I: Paired Samples Statistics Mean N Std. Deviation Std. Error Mean Pair 1 bets1 37.5833 3 9.40771 5.43154 bets2 35.2833 3 8.07927 4.66457 Paired Samples Correlations N Correlation Sig. Pair 1 bets1 & bets2 3 -.521.651 Paired Samples Test Pair 1 bets1 - bets2 Mean 2.300 00 Paired Differences t df Sig. (2- Std. Std. 95% Confidence tailed) Deviati Error Interval of the on Mean Difference Lower Upper 15.2645 9 8.8130 1-35.6193 4 40.2193 4.261 2.819 116

FORMULA II: Pair 1 Paired Samples Statistics Mean N Std. Deviation Std. Error Mean bets1 20.1533 3 2.60231 1.50245 bets2 23.1333 3.83680.48313 Paired Samples Correlations N Correlation Sig. Pair 1 bets1 & bets2 3 -.404.735 Paired Samples Test Pair 1 bets1 - bets2 Mean - 2.98000 Std. Deviation Paired Differences t df Sig. (2- tailed) Std. 95% Confidence Error Interval of the Mean Difference Lower Upper 3.03835 1.75419-10.52769 4.56769-1.699 2.231 FORMULA III: Pair 1 Paired Samples Statistics Mean N Std. Deviation Std. Error Mean bets1 31.3467 3 2.64923 1.52954 bets2 34.1100 3 2.21745 1.28025 117

Paired Samples Correlations N Correlation Sig. Pair 1 bets1 & bets2 3 -.836.369 Paired Samples Test Pair 1 bets1 - bets2 Mean Std. Deviation Paired Differences t df Sig. (2- tailed) Std. 95% Confidence Error Interval of the Mean Difference Lower Upper -2.76333 4.66512 2.69341-14.35213 8.82546-1.026 2.413 ANTAR FORMULA Descriptives persen_pengurangan_penguapan N Mean Std. Deviation Std. Error 95% Confidence Interval for Mean Minimum Maximum Lower Bound Upper Bound formula1 6 36.4333 7.94348 3.24291 28.0972 44.7695 26.23 44.93 formula2 6 21.6433 2.37761.97065 19.1482 24.1385 17.49 24.00 formula3 6 32.7283 2.65801 1.08513 29.9389 35.5177 29.02 36.65 Total 18 30.2683 8.00655 1.88716 26.2868 34.2499 17.49 44.93 Test of Homogeneity of Variances persen_pengurangan_penguapan Levene Statistic df1 df2 Sig. 8.297 2 15.004 118

persen_pengurangan_penguapan Sum of Squares Between Groups ANOVA df Mean Square F Sig. 710.697 2 355.348 14.061.000 Within Groups 379.085 15 25.272 Total 1089.781 17 Multiple Comparisons Dependent Variable: persen_pengurangan_penguapan Tukey HSD (I) formula (J) formula Mean Difference (I-J) Std. Error Sig. 95% Confidence Interval Lower Bound Upper Bound formula formula 2 14.79000 * 2.90243.000 7.2510 22.3290 1 formula 3 3.70500 2.90243.429-3.8340 11.2440 formula formula 1-14.79000 * 2.90243.000-22.3290-7.2510 2 formula 3-11.08500 * 2.90243.004-18.6240-3.5460 formula formula 1-3.70500 2.90243.429-11.2440 3.8340 3 formula 2 11.08500 * 2.90243.004 3.5460 18.6240 *. The mean difference is significant at the 0.05 level. 119

Tukey HSD Formula N Subset for alpha = 0.05 1 2 formula2 6 21.6433 formula3 6 32.7283 formula1 6 36.4333 Sig. 1.000.429 Means for groups in homogeneous subsets are displayed. a. Uses Harmonic Mean Sample Size = 6.000. 120

LAMPIRAN M HASIL UJI STATISTIK UJI DAYA SEBAR ANTAR FORMULA SEDIAAN delta_d N Mean Std. Deviation Descriptives Std. Error 95% Confidence Interval for Mean Lower Upper Bound Bound Minimum Maximum formula1 6 3.9000.22804.09309 3.6607 4.1393 3.50 4.20 formula2 6 4.0667.08165.03333 3.9810 4.1524 4.00 4.20 formula3 6 3.9500.13784.05627 3.8053 4.0947 3.70 4.10 Total 18 3.9722.16735.03945 3.8890 4.0554 3.50 4.20 Test of Homogeneity of Variances delta_d Levene Statistic df1 df2 Sig..513 2 15.609 ANOVA delta_d Sum of Squares df Mean Square F Sig. Between Groups.088 2.044 1.695.217 Within Groups.388 15.026 Total.476 17 121

Dependent Variable: delta_d Tukey HSD (I) formula (J) formula Mean Difference (I-J) formula1 formula2 formula3 Multiple Comparisons Std. Error Sig. 95% Confidence Interval Lower Upper Bound Bound formula2 -.16667.09290.205 -.4080.0746 formula3 -.05000.09290.854 -.2913.1913 formula1.16667.09290.205 -.0746.4080 formula3.11667.09290.440 -.1246.3580 formula1.05000.09290.854 -.1913.2913 formula2 -.11667.09290.440 -.3580.1246 delta_d Tukey HSD formula N Subset for alpha = 0.05 1 formula1 6 3.9000 formula3 6 3.9500 formula2 6 4.0667 Sig..205 Means for groups in homogeneous subsets are displayed. a. Uses Harmonic Mean Sample Size = 6.000. 122

LAMPIRAN N GAMBAR EKSTRAK KERING DAN SEDIAAN HAND BODY LOTION EKSTRAK TEH HIJAU Formula I Formula II Formula III Bets 1 Bets 1 Bets 1 Bets 2 Bets 2 Bets 2 123

LAMPIRAN O GAMBAR RANGKAIAN ALAT UJI EFEKTIFITAS a) b) c) d) a f b e Keterangan: a) Tutup pot plastik yang tidak dilubangi b) Tutup pot plastik yang dilubangi c) Tutup pot plastik yang dilubangi dan tidak dilubangi d) Rangkaian alat uji efektifitas e) Isolasi transparan f) Lengan bawah 124

LAMPIRAN P SERTIFIKAT ANALISIS PEMBELIAN EKSTRAK TEH HIJAU (Camelia sinensis Linn.) 125

LAMPIRAN Q SERTIFIKAT ANALISIS PEMBELIAN KATEKIN HIDRAT 126

LAMPIRAN R SERTIFIKAT ANALISIS PEMBELIAN GLISERIN MONOSTEARAT 127

LAMPIRAN S SERTIFIKAT ANALISIS PEMBELIAN GLISERIN 128

LAMPIRAN T NILAI KRITIS DISTRIBUSI F 129

LAMPIRAN U TABEL KRITIS t 130

LAMPIRAN V HASIL KUISIONER UNTUK UJI HEDONIK Panelis 1 Panelis 2 131

Panelis 3 Panelis 4 132

Panelis 5 Panelis 6 133

Panelis 7 Panelis 8 134

Panelis 9 Panelis 10 135

LAMPIRAN W HASIL KUISIONER UNTUK UJI IRITASI Panelis 1 Panelis 2 136

Panelis 3 Panelis 4 137

Panelis 5 138

Panelis 7 139

Panelis 9 Panelis 10 140